Advances in Photochemistry, Volume 2 by Noyes W

By Noyes W

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Reaction of the (18) type is similar to that of 0 atoms with C&, while a reaction of the (19) type would be similar to known incorporation reactions. The reaction of oxygen atoms with ethyE alcohol was investigated as well. Experiments were carried out using discharges in water vapor and in 02. The results obtained have shown that the CH3CH20Hmolecule displayed properties similar both to those of methyl alcohol and of saturated hydrocarbons, as the CH3CH20H molecule contains the CH, group bound with the C atom (C-C bond).

1 . Experimental Technique Used in Studying the Reactions of Atomic Oxygen with Various Molecules. 35 2. A Method for Determining Oxygen Atom Concentrations. 37 3. Distinction be Consecutive Atom an adical Reactions with Moleculea .... . . . . . . . . . . 39 4. The Mechanism of Reactions between Oxygen Atoms and Various 43 Molecules . . . . . . . . . . . . . . . . . . . . . . . . . . 5. Determination of Rate Constants for Elementary Reactions of Oxygen 53 Atoms with Molecules.

The concentratiop of 0 atoms in samples withdrawn from the flow into the mass spectrometer was twice that of hydroxyl. -'. 2 x 10-13. It does not seem to be very large. This constant is characteristic for the reaction of OH with various hydrocarbons and aldehydes (for example, with CH20). The following conclusion may be drawn from the foregoing: The composition of active speoies removed from the discharge zone in water vapor may change with experinlental conditions. From numerous experiments on discharges in water vapor we came to the conclusion that the main factors influencing the composition of active particles removed from the discharge zone in water vapor were pressure and the condition of the discharge tube and reaction vessel surfaces.

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